• 中国核心期刊（遴选）数据库收录期刊
  • 中国科技论文统计源期刊
  • 中国学术期刊综合评价数据库来源期刊
Advanced Search
YIN Xiangdong, WAn, WANG Jinyu. TiO2 Nano-tube about 30 μm Prepared by Anodic Oxidation[J]. Corrosion & Protection, 2020, 41(11): 61-64. DOI: 10.11973/fsyfh-202011010
Citation: YIN Xiangdong, WAn, WANG Jinyu. TiO2 Nano-tube about 30 μm Prepared by Anodic Oxidation[J]. Corrosion & Protection, 2020, 41(11): 61-64. DOI: 10.11973/fsyfh-202011010
shu

TiO2 Nano-tube about 30 μm Prepared by Anodic Oxidation

  • Shanghai Civil Aviation College, Shanghai 200232, China

More Information
  • Received Date: September 09, 2020
    Graphical Abstract
    • Abstract
  • In order to prepare longer TiO2 nano-tube, Ti sheet was anodically oxidized at direct voltage of 20 V in solution of 0.5(mass fraction)% NaF＋glycerin for 7 h, at the temperature of 0 ℃, 20 ℃ and 40 ℃ respectively. The results of SEM show that the length of the TiO2 nano-tube was 1.034 μm, 2.601 μm and 5.152 μm for 0 ℃, 20 ℃ and 40 ℃ respectively. The results of current density show that balance anodic current density in the solution of 0.5 NaF+glycerin at temperature of 20 ℃ and 40 ℃ was 1.27 mA/cm2 and 1.50 mA/cm2 respectively. At the temperature of 40 ℃, in solution of 0.5% NaF+glycerin, TiO2 nano-tube could grow to about 30 μm for 36 h of anodic oxidation.
    • FullText(HTML)
    • References (21)
  • [1]
    GONG D W,GRIMES C A,VARGHESE O K,et al. Titanium oxide nanotube arrays prepared by anodic oxidation[J]. Journal of Materials Research,2001,16(12):3331-3334.
    [2]
    YANG B. Preparation of bioactive titanium metal via anodic oxidation treatment[J]. Biomaterials,2004,25(6):1003-1010.
    [3]
    RAJA K S,MISRA M,PARAMGURU K. Formation of self-ordered nano-tubular structure of anodic oxide layer on titanium[J]. Electrochimica Acta,2005,51(1):154-165.
    [4]
    MACÁK J M,TSUCHIYA H,SCHMUKI P. High-aspect-ratio TiO2 nanotubes by anodization of titanium[J]. Angewandte Chemie International Edition,2005,44(14):2100-2102.
    [5]
    BERANEK R,HILDEBRAND H,SCHMUKI P. Self-organized porous titanium oxide prepared in H2SO4/HF electrolytes[J]. Electrochemical and Solid-State Letters,2003,6(3):B12.
    [6]
    GOPAL K M,OOMMAN K V,MAGGIE P. A review on highly ordered,vertically oriented TiO2 nanotube arrays:Fabrication,material properties and solar energy applications[J]. Solar Energy Materials & Solar Cells,2006,90:2011-2075.
    [7]
    MACAK J M,SCHMUKI P. Anodic growth of self-organized anodic TiO2 nanotubes in viscous electrolytes[J]. Electrochimica Acta,2006,52(3):1258-1264.
    [8]
    TSUCHIYA H,MACAK J M,GHICOV A,et al. Characterization of electronic properties of TiO2 nanotube films[J]. Corrosion Science,2007,49(1):203-210.
    [9]
    MACÁK J M,TSUCHIYA H,GHICOV A,et al. Dye-sensitized anodic TiO2 nanotubes[J]. Electrochemistry Communications,2005,7(11):1133-1137.
    [10]
    CHEN X B,SCHRIVER M,SUEN T,et al. Fabrication of 10 nm diameter TiO2 nanotube arrays by titanium anodization[J]. Thin Solid Films,2007,515(24):8511-8514.
    [11]
    KANG S H,KIM J Y,KIM H S,et al. Formation and mechanistic study of self-ordered TiO2 nanotubes on Ti substrate[J]. Journal of Industrial and Engineering Chemistry,2008,14(1):52-59.
    [12]
    CRAWFORD G,CHAWLA N,DAS K,et al. Microstructure and deformation behavior of biocompatible TiO2 nanotubes on titanium substrate[J]. Acta Biomaterialia,2007,3(3):359-367.
    [13]
    LAI Y K,SUN L,CHEN C,et al. Optical and electrical characterization of TiO2 nanotube arrays on titanium substrate[J]. Applied Surface Science,2005,252(4):1101-1106.
    [14]
    万斌,沈嘉年,陈鸣波,等. 阳极氧化制备TiO2纳米管及其光催化性能[J]. 化学学报,2008,66(11):1301-1306.
    [15]
    万斌,沈嘉年,陈鸣波,等. 阳极氧化制备TiO2纳米管及其光催化性能[J]. 应用化学,2008,25(6):665-668.
    [16]
    万斌,陈鸣波,周细应,等. Ag/TiO2纳米管的制备及其光催化性能[J]. 稀有金属材料与工程,2009,38(11):2012-2016.
    [17]
    万斌,陈鸣波,周细应,等. Ag/TiO2-xNx纳米管的光电催化性能[J]. 无机材料学报,2010,25(3):285-288.
    [18]
    ZHOU X Y,SHAO J J,WAN B. A one-step electrochemical method for the production of TiO2-xNx Nanotubes[J]. Journal of the Electrochemical Society,2013,160(6):H335-H337.
    [19]
    万斌. Ag,N掺杂对TiO2纳米管电极光催化降解有机染料的影响[J]. 上海:上海大学博士学位论文,2008.
    [20]
    万斌,肖璇,杨琪. 阳极氧化制备10μm长高比表面积的TiO2纳米管[J]. 稀有金属材料与工程,2017,46(8):2318-2321.
    [21]
    MACAK J M,SCHMUKI P. Anodic growth of self-organized anodic TiO2 nanotubes in viscous electrolytes[J]. Electrochimica Acta,2006,52(3):1258-1264.
    • Related Articles

Catalog

    Get Citation
    PDF
    XML
    Article views (1) PDF downloads (3) Cited by()
    Turn off MathJax
    Article Contents
    Abstract
    References

    Corrosion & Protection

    Address：99 Handan Road, ShanghaiPost Code: 200437

    Tel：021-65556775-290Email:cp@mat-test.com

    沪ICP备17055736号-5

    Supported by: Beijing Renhe Information Technology Co., Ltd.  Baidu Analytics

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return